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ACOMP allows comprehensive, model-independent, near realtime monitoring

of many different types of polymerization reactions. It provides conversion kinetics,

and the evolution of average molar mass, intrinsic viscosity and average composition

distributions (for copolymers). Here, recent advances in ACOMP will be summarized,

dealing with continuous reactors, copolymerization, ‘living’ type reactions (NMP,

RAFT, ATRP, ROMP), polyelectrolytes, heterogeneous phase reactions, including free

radical reactions in emulsions, and predictive control. In the case of emulsion

polymerization, a new approach will be presented in which the evolution of the

characteristics of both the soluble phase – monomer conversion, polymer molar mass

and intrinsic viscosity- and the dispersed phase – particle size – are simultaneously

monitored. NSF CBET 0623531, BoR ITRS 019B, NASA NCC3-946, TIMES, PolyRMC (Tulane

Center for Polymer Reaction Monitoring and Characterization).